（转贴）NMR Solvents

renqiang

NMR Solvents

Solvent	Formula	1H shifts	13C shifts	bp °C   z9 q2 ?! K: f2 q. A1 h	mp °C	bp °C
Acetic Acid-d4	CD3COOD	2.0, 11.7	20.0, 180.0	16.6	117.9
Acetone-d6	CD3COCD3	2.09	29.9, 206.7	-94.7	56.1
Acetonitrile-d3	CD3CN	1.94	1.4, 118.7	-43.8	81.6
Benzene-d6	C6D6	7.16	128.4	5.5	80.1
Carbon Disulphide	CS2	none	192.8	-11.6	46.3
Carbon Tetrachloride	CCl4	none	96.7	-23.0	76.8
Chloroform-d	CDCl3	7.24	77.23	-63.5	61.3
Dichloromethane-d2	CD2Cl2	5.32	54.0	-95.1	40.8
Diethyl Ether (-100 °C)	(CH3CH2)2O		?, 66.51	-116.3	34.6
Dimethyl Ether (-100 °C)	CH3OCH3	3.2	60.08	-138.5	-23
N,N-Dimethyl formamide-d7	Me2NCHO	2.95, 2.75, 8.03	29.8, 34.9, 163.2	-61.?	153.?
Dimethyl Sulfoxide-d6	CD3SOCD3 5 [; e) s- X; x	2.50	39.5	18.6	189.0
1,4-Dioxan	(OCH2CH2)2	3.53	66.7	11.8	101.4
Ethanol-d6	CD3CD2OD	1.11, 3.56, 5.19	17.3, 57.0	-117	78.3
Methanol-d4	CD3OD	3.31, 4.78	49.2	-97.8	64.6
Nitrobenzene	C6D5NO2 3 n9 I1 i3 w) `6 b* x7 Y5 ]	7.5, 7.7, 8.1	123, 129, 135	5.7	210.8
Nitromethane-d3 , w, n7 R# k& w	CD3NO2 ( v1 |7 {& r8 E: p7 `- h: Z4 @	4.3	57.3	-28.6	101.2
Pyridine-d5 ! G. O, n4 J/ h; c# D	C5D5N	7.22, 7.58, 8.74	123.9, 135.9, 150.2	-41.6	115.3
1,1,2,2-Tetrachloroethane	CHCl2CHCl2	?	75.5	-43.8	146.3
Tetrahydrofuran-d8 I* g/ n! D% u/ \. E; ?' U- k2 ]	C4D8O	1.73, 3.58	25.4, 67.6	-108.5	65.4
Tetrahydrofuran -100 °C	C4H8O		?, 67.96
Toluene-d8	C6D5CD3	2.09, 6.98, 7.00, 7.09	20.4, 125.5, 128.3, 129.4, 137.9	-94.9	110.6
Trichlorofluoromethane	CFCl3 , }* w6 N2 C$ d4 r! H# I	none	117.6	-111	23.7
Trifluoroacetic Acid-d4 6 T4 }4 {' Y! g" l3 t" T	CF3COOD	11.5	116.6, 164.2	-15.3	72.4
Trifluoroethanol-d3	CF3CD2OD	3.88, 5.02	61.5, 126.3	-15.3	72.4
Water	D2O	4.8	none	0.0	100.0
Solvent	Formula	1H shifts	13C shifts	bp °C   / r& V, R1 b2 B	mp °C	bp °C

yqfeng2001

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figo200066

谢谢阿

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superfluid

* v! A2 W8 Y: p, H% s. ]* Y5 g. ~- C/ r: _7 n+ e/ \, ~7 Z7 W ~, w) ^4 Y P0 \

7 i7 ^* a* E0 z' [! L6 ]7 M( x 谢谢阿 % ]9 S0 O, k8 a+ l5 R+ h M3 w 好东西