1H NMR (THF-d8, 400 MHz): δ 7.29 (dd, J = 8 Hz, 1H), 7.03 (d, J = 8 Hz, 2H), 3.37 (vt, J = 5 Hz, 4H), 1.85 (m, 4H), 1.12 (d of vt, 3JHH = 7 Hz, 3JPH = 7 Hz, 12H), 1.04 (d of vt, 3JHH = 7 Hz, 3JPH = 7 Hz, 12H), ?11.03 (dt, 2JHH = 5 Hz, 2JPH = 17 Hz, 2H), ?21.17 (tt, 2JHH = 5 Hz, 2JPH = 15 Hz, 1H);
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' w/ t! ], W$ Y" ^. q2 t文中说vt是virtual triple,不知道是什么意思?请高手指点迷津 |