gHMQC
3 ?% e& D0 E; g/ n# R; l7 fRelax. delay 1.000 sec " h( W. A3 p3 u3 c
Acq. time 0.160 sec $ ?9 s( U* A9 O' }+ e" [* N# E4 A, O
width 6402.6 Hz
3 o. x8 c. N5 k6 Q* y1 N2D width 17105.0 Hz 1 n% L3 O% c* U$ y# N! _- Q) J
32 repetitions . h5 l4 r% V5 u- M& e7 q+ M2 Q
2×256 increments $ B; i/ v# d( Q( [& _% T) c: f' O
OBSERVE H1, 400.1596234 MHz
) t' V" {* Q: o: Z5 kDECOUPLE C13, 100.6277427 MHz ( Z6 q0 L) h5 p |
POWER 44 dB $ U7 {6 m9 n% R' Z+ O7 d9 {+ x! a
on during acquisition
' T0 f9 g2 j9 Y( |' `off during delay - {; U# O! O2 K4 z4 U {
GARP-1 modulated 1 W$ V* @& q& `. d. @
DATE PROCESSING
0 ~ n! o2 v( z5 [9 g0 T EGauss apodization 0.074 sec ; {3 v% E0 J: O9 d" u
F1 DATE PROCESSING 7 _) W8 X: H* c* R7 g$ z
Gauss apodization 0.014 sec ; R5 F s h4 r. u/ t% w
FT size 2048×2048 % J! y$ C) Z a8 n4 b% U6 C2 s
Total time 5 hr, 33 min,23 sec , N$ B4 R& g, f0 s& U8 ^, U3 n; ]
" p' H% A2 F3 H7 o" l# @
_, W- O2 }* S0 B [
gHMBC 0 w( P! [5 h: W% D3 l
Relax. delay 1.000 sec * P" G0 }2 I; O+ g; J9 d1 T) I$ f+ b
Acq. time 0.160 sec
/ P& [1 O% w! \width 6402.6 Hz / r3 Y; t; e3 }1 F: W B
2D width 24147.3 Hz
E0 |" R9 o8 u% {8 A32 repetitions
1 U. Q& j6 ?2 S4 x0 X# ^2 M" n512 increments
: h, |+ b0 U' w: EOBSERVE H1, 400.1596234 MHz
5 Z4 ]3 B+ E, U0 b% fDATE PROCESSING + K1 G# } K$ v: j: \: J
Sine bell 0.080 sec
! F0 _, @4 `! H+ g, w, s8 Q* HF1 DATE PROCESSING
$ c# L O& b3 I, V6 R% g& F6 L( xSine bell 0.008 sec ! |6 U$ P. T$ [' Z
FT size 2048×2048 2 g+ H# a: w! R% K$ ^
Total time 5 hr, 42 min, 37 sec
/ T5 ?" y( c9 q4 n9 H A2 n6 Y想问一下,从上述参数中可以看出D1指的是什么,还有是弛豫间隔和NS都是什么啊,还有其它参数都是什么意思?不是学这个的,不太懂,还请内行帮忙,先谢谢了 |