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如何学习核磁共振?听北冥给你讲讲。

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发表于 2009-9-24 16:57:52 | 显示全部楼层
北冥有鱼,其实你可以自已这编一本有质量有系统的书啊!!!!!!
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发表于 2009-9-28 23:51:38 | 显示全部楼层
谢谢了
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发表于 2009-10-1 14:38:14 | 显示全部楼层
整个帖子看下来,不得不佩服北冥老师的核磁方面的知识,这个帖子真的值得慢慢看,多次看,慢慢消化。
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发表于 2009-10-2 01:36:46 | 显示全部楼层
 thankssssssssssss
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发表于 2009-10-6 18:43:59 | 显示全部楼层
说的没错,呵呵
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发表于 2009-10-18 13:18:27 | 显示全部楼层

好强大啊..

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发表于 2009-10-18 20:29:13 | 显示全部楼层
我现在也刚刚在学习如何解析核磁谱图,想问一下谱图峰强度低是怎么回事啊!
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发表于 2009-10-20 23:02:35 | 显示全部楼层
 介绍一本新书 Classics in Spectroscopy (2009)



 

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发表于 2009-10-20 23:05:50 | 显示全部楼层
http://www.wiley.com/WileyCDA/WileyTitle/productCd-3527325166,descCd-authorInfo.html

Description:
Classics in Spectroscopy: Isolation and Structure Elucidation of Natural Products
- j1 H0 B1 g3 ~2 C# e) o2 d0 g" ` is the first book of its kind to describe the art of NMR using everyday2 E3 o# \2 O4 m' m N examples. This textbook will not only fascinate students wanting to ) l' f' G v$ O) plearn about the topic, but also those experienced analytical chemists5 S# Y3 s- i: E who are still inspired by their profession. + d4 S' t, P/ y; f6 E* M# T

The contents provide for easy reading by using natural products * T! Y- A: r$ F/ Athat everyone knows, such as caffeine, backed by an attractive layout 2 |7 L0 l- W2 t) I/ r6 {$ D' X% S5 hwith many pictures to visualize the topics.; {5 V8 N( r6 J

In addition, an in-depth analytical part makes the book a0 O0 u) A' \3 {; u0 B, c6 b: U valuable teaching tool, or for self-learning using the questions and " J5 X- F7 m- r7 o# v1 Y6 Q. i6 B- ]; ~( uanswers at the end of each chapter.


Table of Contents:

Preface. ; Z& }7 N7 c8 a& S , v, x% ?& M% T$ s* d H. D, D

% ~- z% W, v" T; O& U; S* |3 O ALKALOIDS. 5 M/ u( g' F( R) I1 a" f" n' l2 r8 S$ R" X: V" T" n

1 f0 q4 x9 W0 a* s! o" y) g1 ?& C Nicotine. + P; W) \: _& e* G9 U$ d2 ~ , _7 r, }: d6 l

- ~+ R. O9 W* s/ J5 z) f Caffeine. 2 C4 ?; k1 Y& f4 F- X" g4 u" d, P. G/ I# N6 d9 U; S6 p

/ Z. b0 p9 y1 f4 K/ i* M0 Y# [Theobromine. ! W8 J5 }% k2 o' \3 {: R. ^; p% P7 R/ _

! q* ]. `% w+ a% p& D Piperine. % O: ^/ T( B. [# a 3 f- ? o8 K0 P2 `! I

$ _) o0 T) P1 ^& u% ] Cytisine.5 r& X8 T- j# d8 X4 C: n 1 c4 q, ]5 K S# w8 s( [2 ?) ^, w

7 S* W% h( p2 ?) ], a Galanthamine.: q% t( z4 Q* J" g; T0 r# Z7 H( H # |3 f( T" G v9 P; w1 |

& [3 l, ^. w9 B, IStrychnine." Z% |1 [* c, n8 f8 F. O ) z( h; w2 Q9 E0 v4 `

" D* m$ u# Q k4 k( S( T, q" h AROMATIC COMPOUNDS.& |7 ~! F& U( s7 T " `! ?& h5 |) Y+ {& D4 O0 [

$ ?, R& i. S) O6 S) P# P Anethole. 4 f* a- X( X( U6 P8 w0 C - z9 r/ t9 U* V: z! p

2 d. P& ?3 _9 f( u P. x Eugenol. ! K2 f" d/ ]1 B1 m 0 N% y" [0 d7 D7 u

* j6 W& U0 N4 X% c" L% k1 pChamazulene. 2 M- i6 `! c/ I8 C . \# {; t6 G; P" ]- [$ B

2 p2 P& [7 \* e1 g6 }Tetrahydrocannabinol. " S8 f2 `+ H5 s* m ! z2 G4 O/ I. \/ \8 l/ ^4 B

% K9 ?" g& R; c- U0 }, x: _DYESTUFFS AND COLOURED COMPOUNDS. . A8 O/ I0 F( e3 P* O4 f* b; c% H4 G

0 S1 t# y' B% B. P$ S8 d! K# R Lawsone. % Q- D% h6 g5 h1 n4 K 2 g1 ^7 {6 _7 a+ ?2 y. j

; `& ^2 E' y* ~* Q3 Q& ZCurcumin. - z L. e N4 A. K# M. I ' L9 k U' r0 V1 c; Z

0 N+ j" o, v& t d5 ^( I Brazileine. ! ]5 \( S6 k }7 z" m$ I0 [/ G2 d' D. _6 p' t

8 v1 V) U: t3 D9 F6 N7 n+ n) b: dIndigo.3 H% Y5 e n8 L% w) c S" ] 5 t1 M- z+ i; p6 i; M2 y! T

n* { O4 C, |3 `% }: ?Capsanthin. 9 P \+ l8 ~1 Z) V6 I+ \8 t& N' D( A, C: h& w8 H& O/ o1 O/ B

1 {' a1 c S) o% e" q7 ` CARBOHYDRATES. # m4 f/ o0 G0 c7 A7 l , M% k+ W/ y; W; e L

$ O9 h7 Y: S7 V. ?. o. A+ G5 sGlucosamine. 2 a$ `9 C2 R+ F6 J4 `# ^$ k4 _( L3 P3 M- S$ s0 \4 z

& n3 O" M; U, u0 gLactose.+ U v4 a, z: F& y6 V / D2 @ R& N# l1 y8 Q% t

# i# b% `- s' a5 N4 l0 R- S. yAmygdalin.! u9 ?; Y& O, A7 [3 Y ( f+ D- {: p5 J/ n1 w

2 W# K: F" i5 f. |: g3 z% qHesperidin., N( g, R; K- H 7 x2 \( F( Y) _* j1 [* |; p

& V; a I, Q- x" s TERPENOIDS. : l4 r" K; m! P% { . ^2 a5 `: T( C: b# i1 ]3 |

% \ `, z# P: Y1 t: D7 ULimonene. ' V0 j+ C( I$ x. _( B" b3 z l3 s * f! f4 W, a$ ~: Z# ?' @ {' Q

( H- j* ~8 a0 `/ C% ~Menthol.3 W& b* C2 P; [) H( K # N- G$ U" c' P, ~# i+ ?) V

9 } M9 R; C2 I4 T, nThe Thujones.5 O# ^' q5 P: r7 H 5 `3 u3 G5 L1 \3 @3 p) }( ~

- {. ?, N8 ^8 g' G kPatchouli Alcohol. ! Y6 F8 E1 ^7 ?4 y1 I6 B / X5 D4 g) Z4 O

8 b% }! @- F5 z; ] e# POnocerin. 3 K; v: @7 z( q! W. f5 M$ P# H2 T+ u' B/ W5 t9 E e" A6 v

3 @* i4 l$ u0 l. A6 V Cnicin. 1 X" F- i7 J/ q7 k" f) x 9 y9 H" k0 I1 O0 L& N

. k9 c! R% i1 h/ V1 Q' O3 X Abietic Acid. 9 k" M9 g0 k9 t# }4 L( k3 K/ h# X5 D1 L; r f5 T! {9 Z6 }2 [9 }( x

8 e8 z) X: m% I FBetulinic Acid. 6 F! k2 E9 F, F% h2 [" A9 H* A. n0 b2 X- s. ^% v2 y

: E" \7 T- J, s$ W' V; ZMISCELLANEOUS. : }# O) n2 A! N/ y9 H5 T! k! m: X& J' m% {& ^4 D# U

# n" h l5 w& f4 X( _* d Shikimic Acid.+ ^ s$ s+ k+ i7 N. }5 G * S6 ?, Q- x1 A3 `9 L: l

" K6 A& ? }8 o" v% d Aleuritic Acid. Y C9 Q2 Z1 {& Y. r% t3 N7 w 5 F, T% \) @0 S( ~) Y8 S* p

a y* D2 G( X. N" w+ T( CANSWERS TO QUESTIONS AND TRANSLATIONS. 1 k2 S X& C0 x" e% f* Z! B* |- V H) e3 y6 [) t, u

- U1 a* d% _) n w: c Appendix.


Author Information:

Stefan Berger
is 8 y0 a8 s5 l3 j7 \. Oprofessor for structural analytics at the University of Leipzig.; C6 P5 S* A- ]; u Besides his many publications he wrote and edited several books among4 q J+ A: t$ G' ?$ \1 g3 G$ H# b them 100/150/200 and more basic NMR Experiments, NMR Spectroscopy of2 C3 M$ L2 J3 ` non-metals, and 13C-NMR-Spectroscopy. 0 m; k* K5 ]7 E) W, Y/ B) U* I/ g

* b1 f# j7 Q3 D& X$ ?+ c Dieter Sicker is adjunct professor at the University of Leipzig.6 g$ O/ Q9 c, O His current research involves him in natural product and heterocycles! I/ Q7 k7 A0 c7 Z synthesis and carbohydrate chemistry. / k6 F' n6 m; A j


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发表于 2009-10-20 23:08:32 | 显示全部楼层
"describe the art of NMR using everyday y5 ]3 \7 t; M6 y examples!"--- 网上有电子版.


, k6 h6 g7 N5 H) K9 u
[此贴子已经被作者于2009-10-20 23:12:20编辑过]
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