[推荐]11B NMR实验参数和化学位移以及文献

celan

11B NMR实验参数

[此贴子已经被作者于2007-11-20 17:39:01编辑过]

celan

化学位移，参照物

[此贴子已经被作者于2007-11-20 17:26:00编辑过]

+ o% `* t9 O! B8 i4 v2 F4 a/ a3 O

celan

Boron-11 NMR文献

"Boron-11 NMR," W. G. Henderson and E. F. Mooney, Ann. Rev. NMR Spectr.1969, 2, 219; 1982, 12, 177.

"¹¹B NMR Spectroscopy," A. R. Siedle, Ann. Rep. NMR Spect. 1988, 20, 205.

"NMR Spectroscopy of Boron Compounds Containing two-, three- and four-Coordinate Boron," B. Wrackmeyer, Ann. Rep. NMR Spect. 1988, 20, 61.

"The Role of NMR in Boron Chemistry," Reed, D. Chem. Soc. Rev. 1993, 22, 109.

"Nuclear Magnetic Resonance Spectroscopy of Boron Compounds," H. Noth and B. Wrackmeyer, Springer-Verlag, NY, 1978.

"NMR of Boron Compounds," H. Nöth and B. Wrackmeyer, QC/490/N2.

celan

一个11B NMR
4 F% J! e/ T4 Q6 ?+ b

[此贴子已经被作者于2007-11-20 17:45:23编辑过]

B5 x) W% P) \& \

celan

boron properties NMR observation frequencies in MHz for each magnetic field value found in NMR magnets at NHMFL: MHz 200 300 400 500 600 720 750 830 900 1065 11B 64.2 96.3 128 160 193 231 241 266 289 341.4 10B 21.5 32.2 43 53.7 64.5 77.4 80.6 89.2 96.7 114.3 Tesla 4.70 7.05 9.40 11.7 14.1 16.9 17.6 19.6 21.2 25.0 Other properties: spin gamma abundance sensitivity abs. sens-ty chem. shift 11B 3/2 8.583e7 80.42 0.17 0.137 10B 3 2.875e7 19.58 0.0199 0.0039   rad/T percent     ppm

laome5000

谢谢！

非常好

[em01]

arieszj

请教您一下

如果我想做11B-11B cosy

channel 和 parameter应该怎么设呢

我用的是bruker 300MHz的机器，pulse program 用的是cosyqf45

多谢

titus

有几篇文献不错 适合下载阅读